Database survey

A search of the Cambridge Structural Database (Version XX, update February XX; Groom et al. , 2016) for the substructure of 2-(alkylthio)isoindoline-1,3-dione yielded XX hits.

Synthesis and crystallization

Compound (I) was prepared by a similar procedure to Reese et al. 

Refinement details

Crystal data, data collection and structure refinement details are summarized in Table X. All hydrogen atoms are placed in calculated positions [C—H = 0.98–0.99 Å; U iso(H) = 1.2 or 1.5U eq(C)].