REFERENCES
1. Nisperos-Carriedo, M. O.; Baldwin, E. A.; Moshonas, M. G.; Shaw, P. E., Determination of volatile flavor components, sugars, and ascorbic, dehydroascorbic, and other organic acids in calamondin (Citrus mitis Blanco). Journal of Agricultural & Food Chemistry 1993, 40 (12), 2464-2466.
2. Moshonas, M. G.; Shaw, P. E., Volatile Components of Calamondin Peel Oil. Journal of Agricultural & Food Chemistry 1996, 44 (4), 1105-1107.
3. Lou, S. N.; Hsu, Y. S.; Ho, C. T., Flavonoid compositions and antioxidant activity of calamondin extracts prepared using different solvents. Journal of Food & Drug Analysis 2014, 22 (3), 290-295.
4. Manaf, Y. N. A.; Osman, A.; Lai, O. M.; Long, K.; Ghazali, H. M., Characterisation of musk lime (Citrusmicrocarpa) seed oil. Journal of the Science of Food and Agriculture 2008, 88 (4), 676-683.
5. Castillo-Herrera, G. A.; Farías-Álvarez, L. J.; García-Fajardo, J. A.; Delgado-Saucedo, J. I.; Puebla-Pérez, A. M.; Lugo-Cervantes, E., Bioactive extracts of Citrus aurantifolia swingle seeds obtained by supercritical CO 2 and organic solvents comparing its cytotoxic activity against L5178Y leukemia lymphoblasts. Journal of Supercritical Fluids 2015,101 , 81-86.
6. Lou, S. N.; Ho, C. T., Phenolic compounds and biological activities of small-size citrus: Kumquat and calamondin. Journal of food and drug analysis 2017,25 (1), 162-175.
7. Moulehi, I.; Bourgou, S.; Ourghemmi, I.; Tounsi, M. S., Variety and ripening impact on phenolic composition and antioxidant activity of mandarin (Citrus reticulate Blanco) and bitter orange (Citrus aurantium L.) seeds extracts.Industrial Crops & Products 2012, 39 (1), 74-80.
8. Jorge, N.; Silva, A. C. D.; Aranha, C. P. M.; Jorge, N.; Silva, A. C. D.; Aranha, C. P. M., Antioxidant activity of oils extracted from orange (Citrus sinensis) seeds.Anais Da Academia Brasileira De Ciencias 2016, 88(2), 951-958.
9. El‐Adawy, T. A.; El‐Bedawy, A. A.; Rahma, E. H.; Gafar, A. M., Properties of some citrus seeds. Part 3. Evaluation as a new source of protein and oil. Molecular Nutrition & Food Research 1999, 43 (6), 385-391.
10. Hosamani, K. M.; Sattigeri, R. M., Industrial utilization of Rivea ornata seed oil: a moderate source of vernolic acid. Industrial Crops & Products 2000,12 (2), 93-96.
11. Ajewol, K.; Adeyeye, A., Characterisation of Nigerian citrus seed oils. Food Chemistry1993, 47 (1), 77-78.
12. Habib, M. A.; Hammam, M. A.; Sakr, A. A.; Ashoush, Y. A., Chemical evaluation of egyptian citrus seeds as potential sources of vegetable oils. Journal of the American Oil Chemists’ Society 1986, 63 (9), 1192-1196.
13. Saloua, F.; Eddine, N. I.; Hedi, Z., Chemical composition and profile characteristics of Osage orange Maclura pomifera (Rafin.) Schneider seed and seed oil. Industrial Crops & Products 2009, 29 (1), 1-8.
14. Yilmaz, E.; Güneşer, B. A., Cold pressed versus solvent extracted lemon ( Citrus limon L.) seed oils: yield and properties. Journal of Food Science & Technology2017, 54 (7), 1891.
15. Anwar, F.; Naseer, R.; Bhanger, M. I.; Ashraf, S.; Talpur, F. N.; Aladedunye, F. A., Physico-Chemical Characteristics of Citrus Seeds and Seed Oils from Pakistan.Journal of the American Oil Chemists’ Society 2008,85 (4), 321-330.
16. Waheed, A.; Mahmud, S.; Saleem, M.; Ahmad, T., Fatty acid composition of neutral lipid: Classes of Citrus seed oil. Journal of Saudi Chemical Society 2009,13 (3), 269-272.
17. Saïdani, M.; Dhifi, W.; Marzouk, B., Lipid evaluation of some Tunisian citrus seeds. Journal of Food Lipids 2010, 11 (3), 242-250.
18. Matthaus, B.; Özcan, M. M., Chemical evaluation of citrus seeds, an agro-industrial waste, as a new potential source of vegetable oils. Grasas y Aceites2012, 63 (3), 313-320.
19. İnan, Ö.; Özcan, M. M.; Aljuhaimi, F., Effect of location and Citrus
species on total phenolic, antioxidant, and radical scavenging activities of some Citrus
seed and oils. Journal of Food Processing and Preservation2018, 42 (3), e13555.
20. Oyekunle, J. A. O.; Omode, A. A., Chemical composition and fatty acid profile of the lipid fractions of selected Nigerian indigenous oilseeds. International Journal of Food Properties 2008, 11 (2), 273-281.
21. Moreno, A. O.; Dorantes, L.; Galíndez, J.; Guzmán, R. I., Effect of different extraction methods on fatty acids, volatile compounds, and physical and chemical properties of avocado (Persea americana Mill.) oil. Journal of Agricultural & Food Chemistry 2003, 51 (8), 2216-21.
22. China, S. a. o., Inspection of vegetable oils methods for determination of specific gravity. Standardization administration of China 1985; Vol. GB5526-1985.
23. China, S. a. o., Animal and vegetable fats and oils-Determination of refractive index. Standardization administration of China 2010; Vol. GB/T 5527-2010.
24. China, S. a. o., Animal and vegetable fats and oils-Determination of Lovibond colour. Standardization administration of China 2008; Vol. GB/T22460-2008.
25. China, S. a. o., Animal and vegetable fats and oils-Determination of acid value and acidity. Standardization administration of China 2005; Vol. GBT/5530-2005.
26. China, S. a. o., Animal and vegetable fats and oils - Determination of peroxide value. Standardization administration of China 2005; Vol. GB/T5538-2005.
27. China, S. a. o., Animal and vegetable fats and oils- Determination of iodine value. Standardization administration of China 2008; Vol. GB/T5532-2008.
28. China, S. a. o., Animal and vegetable fats and oils - Determination of saponification value. Standardization administration of China 2008; Vol. GB/T5534-2008.
29. China, S. a. o., Animal and vegetable fats and oils - Determination of unsaponifiable matter- Part 1: Method using diethyl ether extraction. Standardization administration of China 2008; Vol. GB/T5535.1-2008.
30. Carreau, J. P.; Dubacq, J. P., Adaptation of a macro-scale method to the micro-scale for fatty acid methyl transesterification of biological lipid extracts. Journal of Chromatography A 1978, 151 (3), 384-390.
31. Carasek, E.; Pawliszyn, J., Screening of tropical fruit volatile compounds using solid-phase microextraction (SPME) fibers and internally cooled SPME fiber.Journal of Agricultural & Food Chemistry 2006,54 (23), 8688-96.
32. China, S. G. A. o., Inspection of grain and oils- Determination of polyphenols in vegetable oil - Spectrometric method. the State Grain Administration of China: 2017; Vol. LS/T 6119-2017.
33. Chinapongtitiwat, V.; Jongaroontaprangsee, S.; Chiewchan, N.; Devahastin, S., Important flavonoids and limonin in selected Thai citrus residues. Journal of Functional Foods 2013, 5 (3), 1151-1158.
34. Marinova, D.; Ribarova, F.; Atanassova, M., Total phenolics and total flavonoids in Bulgarian fruits and vegetables. Journal of the university of chemical technology and metallurgy 2005, 40 (3), 255-260.
35. Lerma-Garcia, M. J.; Simo-Alfonso, E. F.; Mendez, A.; Lliberia, J. L.; Herrero-Martinez, J. M., Fast separation and determination of sterols in vegetable oils by ultraperformance liquid chromatography with atmospheric pressure chemical ionization mass spectrometry detection. Journal of agricultural and food chemistry 2010, 58 (5), 2771-6.
36. Pradhan, R. C.; Meda, V.; Rout, P. K.; Naik, S.; Dalai, A. K., Supercritical CO2 extraction of fatty oil from flaxseed and comparison with screw press expression and solvent extraction processes. Journal of Food Engineering 2010,98 (4), 393-397.
37. Kiralan, M.; Özkan, G.; Bayrak, A.; Ramadan, M. F., Physicochemical properties and stability of black cumin (Nigella sativa) seed oil as affected by different extraction methods. Industrial Crops and Products 2014, 57 , 52-58.
38. Ixtaina, V. Y.; Martínez, M. L.; Spotorno, V.; Mateo, C. M.; Maestri, D. M.; Diehl, B. W. K.; Nolasco, S. M.; Tomás, M. C., Characterization of chia seed oils obtained by pressing and solvent extraction. Journal of Food Composition and Analysis 2011, 24 (2), 166-174.
39. Ndayishimiye, J.; Getachew, A. T.; Chun, B. S., Comparison of Characteristics of Oils Extracted from a Mixture of Citrus Seeds and Peels Using Hexane and Supercritical Carbon Dioxide. Waste and Biomass Valorization 2016, 8(4), 1205-1217.
40. Bennett, R. D.; Hasegawa, S., 7α-Oxygenated limonoids from the rutaceae. Phytochemistry1982, 21 (9), 2349-2354.
41. Champagne, D. E.; Koul, O.; Isman, M. B.; Gge, S.; Ghn, T., Biological activity of limonoids from the Rutales. Phytochemistry 1992, 31 (2), 377-394.
42. Bilal, H.; Akram, W.; Hassan, S. A.; Sahar, S.; Iqbal, M. M., Determination of limonin and nomilin contents in different citrus cultivars using high performance liquid chromatography. Biological Sciences-PJSIR 2013,56 (1), 36-40.
43. Herent, M. F.; De Bie, V.; Tilquin, B., Determination of new retention indices for quick identification of essential oils compounds. Journal of pharmaceutical and biomedical analysis 2007, 43 (3), 886-92.
44. de Moraes Pultrini, A.; Galindo, L. A.; Costa, M., Effects of the essential oil from Citrus aurantium L. in experimental anxiety models in mice. Life sciences2006, 78 (15), 1720-1725.
45. Lou, S. N.; Hsu, Y. S.; Ho, C. T., Flavonoid compositions and antioxidant activity of calamondin extracts prepared using different solvents. Journal of food and drug analysis 2014, 22 (3), 290-295.
46. Ogbunugafor, H.; Eneh, F.; Ozumba, A.; Igwo-Ezikpe, M.; Okpuzor, J.; Igwilo, I.; Adenekan, S.; Onyekwelu, O., Physico-chemical and antioxidant properties of Moringa oleifera seed oil. Pakistan Journal of Nutrition 2011,10 (5), 409-414.
47. Malacrida, C. R.; Kimura, M.; Jorge, N., Phytochemicals and antioxidant activity of citrus seed oils.Food Science and Technology Research 2012, 18(3), 399-404.
48. Kalua, C.; Allen, M.; Bedgood Jr, D.; Bishop, A.; Prenzler, P. D.; Robards, K., Olive oil volatile compounds, flavour development and quality: A critical review.Food Chemistry 2007, 100 (1), 273-286.
Table 1 Physicochemical properties of Qingjinju seed oils obtained using different extraction methods